Full Report Set



  ASAP 2020 V3.01 H    Unit 1    Serial #: 220    Page  1  

     Sample:    WTO129-3.SMP                      
   Operator:                                      
  Submitter:                                      
       File:    C:\2020\DATA\DUMELE\WTO129-3.SMP  

            Started:    09.12.2021 15:11:08       Analysis Adsorptive:    N2                    
          Completed:    09.12.2021 15:09:56       Analysis Bath Temp.:    -195.802 C           
        Report Time:    11.12.2021 14:30:36        Thermal Correction:    No                    
        Sample Mass:    0.0412 g                      Warm Free Space:    15.8692 cm Measured  
    Cold Free Space:    48.2697 cm            Equilibration Interval:    45 s                  
  Low Pressure Dose:    0.5000 mmol/g                 Automatic Degas:    No                    







                      Isotherm Tabular Report

   Relative       Absolute      Quantity    Elapsed    Saturation   
   Pressure       Pressure      Adsorbed     Time       Pressure    
    (p/p)         (mbar)       (mmol/g)    (h:min)      (mbar)     
-----
  1.#QNAN0000       1.#QNAN0     1.#QNAN      00:58    1016.821236  
  0.000009499       0.009655     0.51367      01:56       1.#QNAN0  
  0.000015258       0.015504     1.02506      02:48       1.#QNAN0  
  0.000032291       0.032801     1.53127      03:39       1.#QNAN0  
  0.000057920       0.058813     2.02986      04:34       1.#QNAN0  
  0.000095212       0.096643     2.51761      05:35       1.#QNAN0  
  0.000146514       0.148652     2.99054      06:42       1.#QNAN0  
  0.000213711       0.216720     3.44413      08:02       1.#QNAN0  
  0.000299553       0.303605     3.87278      09:27       1.#QNAN0  
  0.000404458       0.409715     4.27081      10:49       1.#QNAN0  
  0.000589002       0.596440     4.77462      11:46       1.#QNAN0  
  0.000841709       0.852038     5.27412      12:41       1.#QNAN0  
  0.001183541       1.197475     5.76794      13:58       1.#QNAN0  
  0.001660646       1.679692     6.25233      14:45       1.#QNAN0  
  0.002301500       2.326988     6.72527      15:46       1.#QNAN0  
  0.003160530       3.194468     7.18183      16:38       1.#QNAN0  
  0.004312476       4.357276     7.63376      17:32       1.#QNAN0  
  0.005771249       5.829261     8.06777      18:24       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      18:32    1010.000100  
  0.007653306       7.729442     8.49620      18:44       1.#QNAN0  
  0.009577698       9.672522     8.85466      18:55       1.#QNAN0  
  0.012045787      12.164785     9.25059      19:00       1.#QNAN0  
  0.013026927      13.155392     9.39637      19:04       1.#QNAN0  
  0.013301706      13.432708     9.43871      19:07       1.#QNAN0  
  0.014158073      14.297081     9.56360      19:14       1.#QNAN0  
  0.015884819      16.040574     9.78556      19:17       1.#QNAN0  
  0.017021317      17.187847     9.93377      19:22       1.#QNAN0  
  0.018268531      18.446868    10.09260      19:27       1.#QNAN0  
  0.020612040      20.812896    10.36996      19:31       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      19:34    1009.731648  
  0.023335189      23.562546    10.68321      19:38       1.#QNAN0  
  0.027210197      27.475543    11.04356      19:41       1.#QNAN0  
  0.029504268      29.792407    11.29898      19:46       1.#QNAN0  
  0.030765808      31.066709    11.43427      19:51       1.#QNAN0  
  0.034794372      35.135173    11.84162      19:56       1.#QNAN0  
  0.039475123      39.862449    12.30207      20:02       1.#QNAN0  
  0.045135492      45.579133    12.82367      20:08       1.#QNAN0  
  0.051212670      51.716777    13.34390      20:13       1.#QNAN0  
  0.051774865      52.285100    13.40148      20:17       1.#QNAN0  
  0.052690470      53.210333    13.48444      20:21       1.#QNAN0  
  0.053698841      54.229114    13.56516      20:24       1.#QNAN0  
  0.054704652      55.245485    13.64755      20:28       1.#QNAN0  
  0.055709703      56.260950    13.72886      20:31       1.#QNAN0  
  0.056848078      57.411404    13.82228      20:36       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      20:38    1009.915064  
  0.058274049      58.853669    13.93068      20:42       1.#QNAN0  
  0.059674985      60.270412    14.03870      20:46       1.#QNAN0  
  0.061324751      61.938565    14.16241      20:50       1.#QNAN0  
  0.063107019      63.740653    14.29141      20:54       1.#QNAN0  
  0.064934466      65.588997    14.41928      20:59       1.#QNAN0  
  0.066959868      67.636391    14.55372      21:02       1.#QNAN0  
  0.068843871      69.541589    14.67825      21:06       1.#QNAN0  
  0.070893283      71.613441    14.81188      21:09       1.#QNAN0  
  0.073156369      73.902387    14.95651      21:14       1.#QNAN0  
  0.075402774      76.174066    15.09056      21:18       1.#QNAN0  
  0.079973427      80.793983    15.34700      21:22       1.#QNAN0  
  0.085854694      86.738289    15.65471      21:26       1.#QNAN0  
  0.096976985      97.978853    16.19049      21:31       1.#QNAN0  
  0.099868372     100.902461    16.32329      21:34       1.#QNAN0  
  0.111139739     112.294899    16.81835      21:39       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      21:42    1010.417302  
  0.126049944     127.352380    17.45859      21:47       1.#QNAN0  
  0.139557487     140.987685    18.05721      21:52       1.#QNAN0  
  0.142897280     144.352033    18.21654      21:56       1.#QNAN0  
  0.161251463     162.876698    19.16035      22:02       1.#QNAN0  
  0.179595351     181.381162    20.55734      22:10       1.#QNAN0  
  0.206786589     208.804288    24.48294      22:21       1.#QNAN0  
  0.237577461     239.879519    24.87915      22:25       1.#QNAN0  
  0.254796532     257.252504    25.06413      22:28       1.#QNAN0  
  0.278138785     280.800927    25.30654      22:32       1.#QNAN0  
  0.301675310     304.547413    25.56157      22:35       1.#QNAN0  
  0.314991744     317.974636    25.69053      22:38       1.#QNAN0  
  0.352369600     355.688564    25.89468      22:41       1.#QNAN0  
  0.374171647     377.683302    25.99617      22:43       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      22:46    1009.334383  
  0.400651739     404.397582    26.11675      22:48       1.#QNAN0  
  0.404235394     408.023831    26.13976      22:51       1.#QNAN0  
  0.450520483     454.752828    26.30816      22:54       1.#QNAN0  
  0.478348701     482.849645    26.40764      22:56       1.#QNAN0  
  0.500308691     505.027513    26.48391      22:59       1.#QNAN0  
  0.523550128     528.496007    26.56263      23:01       1.#QNAN0  
  0.550150208     555.355621    26.64638      23:03       1.#QNAN0  
  0.595679982     601.325118    26.78010      23:05       1.#QNAN0  
  0.599970768     605.670058    26.80604      23:08       1.#QNAN0  
  0.650809685     657.001663    26.94674      23:10       1.#QNAN0  
  0.695557669     702.191032    27.08013      23:13       1.#QNAN0  
  0.700054212     706.740952    27.10522      23:15       1.#QNAN0  
  0.740803562     747.896187    27.23348      23:18       1.#QNAN0  
  0.772685268     780.094718    27.34937      23:20       1.#QNAN0  
  0.807423358     815.178023    27.49855      23:22       1.#QNAN0  
  0.873252086     881.665165    27.89978      23:26       1.#QNAN0  
  0.913560165     922.382122    28.40693      23:29       1.#QNAN0  
  0.926162528     935.127008    28.67589      23:32       1.#QNAN0  
  0.946498697     955.688391    29.32531      23:36       1.#QNAN0  
  0.953346984     962.631751    29.68020      23:40       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      23:50    1009.814080  
  0.987424304     997.183361    34.88392      23:58       1.#QNAN0  
  0.992560283    1002.456041    37.54123      24:08       1.#QNAN0  
  0.983872544     993.732798    36.15707      24:14       1.#QNAN0  
  0.976196046     986.046986    34.31673      24:22       1.#QNAN0  
  0.968821314     978.664941    32.90420      24:30       1.#QNAN0  
  0.960625038     970.443610    31.71897      24:37       1.#QNAN0  
  0.950020311     959.788072    30.69534      24:44       1.#QNAN0  
  0.936539435     946.217244    29.82433      24:50       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      24:52    1010.350901  
  0.920246331     929.684420    29.18439      24:56       1.#QNAN0  
  0.901165566     910.322483    28.70942      25:00       1.#QNAN0  
  0.875556616     884.370265    28.31259      25:04       1.#QNAN0  
  0.858371608     866.951202    28.12583      25:07       1.#QNAN0  
  0.840996355     849.362394    27.97592      25:09       1.#QNAN0  
  0.820766134     828.872538    27.84053      25:12       1.#QNAN0  
  0.800861570     808.733402    27.72908      25:14       1.#QNAN0  
  0.770868492     778.390675    27.58979      25:17       1.#QNAN0  
  0.740846292     748.040381    27.47299      25:19       1.#QNAN0  
  0.700978340     707.735418    27.33562      25:22       1.#QNAN0  
  0.650961091     657.189718    27.17910      25:25       1.#QNAN0  
  0.600895390     606.616472    27.03259      25:27       1.#QNAN0  
  0.550908783     556.114755    26.88641      25:30       1.#QNAN0  
  0.501005664     505.704419    26.73260      25:33       1.#QNAN0  
  0.451633830     455.837415    26.47921      25:36       1.#QNAN0  
  0.399087936     402.774058    26.28650      25:39       1.#QNAN0  
  0.351802364     355.026712    26.08520      25:42       1.#QNAN0  
  0.301433690     304.167805    25.76870      25:46       1.#QNAN0  
  0.251524664     253.782228    25.25341      25:50       1.#QNAN0  
  0.200701581     202.483944    24.51819      25:54       1.#QNAN0  
  1.#QNAN0000       1.#QNAN0     1.#QNAN      25:57    1008.809523  
  0.145836565     147.376728    18.65331      26:10       1.#QNAN0  
  0.100265462     101.445925    16.59502      26:19       1.#QNAN0  
  0.070409088      71.313925    15.00996      26:27       1.#QNAN0  


 Options Report


              Sample Tube

         Warm freespace:    1.0000 cm  
         Cold freespace:    1.0000 cm  
    Non-ideality factor:    0.0000620   
  Use Isothermal Jacket:    Yes         
         Use Filler Rod:    Yes         
       Vacuum seal type:    Seal Frit   

 Analysis Conditions


                 Preparation

               Fast evacuation:    No        
  Unrestricted evacuation from:    6.7 mbar  
               Vacuum setpoint:    13 bar   
               Evacuation time:    0.10 h    
                     Leak test:    No        
                 Use TransSeal:    No        

                Free Space

             Free-space type:    Measured  
  Lower dewar for evacuation:    Yes       
             Evacuation time:    0.10 h    
                 Outgas test:    No        

                                                       p and Temperature

         p and T type:    Measure p at intervals during analysis.  Calculate the Analysis Bath Temperature from these values.  
  Measurement interval:    60 min                                                                                                

                         Dosing

  Use first pressure fixed dose:    No                  
   Use maximum volume increment:    No                  
               Target tolerance:    5.0% or 6.666 mbar  
            Low pressure dosing:    Yes                 
                    Dose amount:    0.50000 mmol/g      
    Minimum equilibration delay:    0.00 h              
    Maximum equilibration delay:    999.00 h            

                      Equilibration

       Equilibration time (p/p = 0.010000000):    45 s   
       Equilibration time (p/p = 1.000000000):    10 s   
  Minimum equilibration delay at p/p >= 0.995:    600 s  

             Sample Backfill

  Backfill at start of analysis:    Yes  
    Backfill at end of analysis:    Yes  
                   Backfill gas:    N2   

                Adsorptive Properties

                         Adsorptive:    Nitrogen      
          Maximum manifold pressure:    1233.23 mbar  
                Non-ideality factor:    0.0000620     
          Density conversion factor:    0.0015468     
  Therm. tran. hard-sphere diameter:    0.386 nm      
     Molecular cross-sectional area:    0.162 nm     


  Inside diameter of sample tube:    9.53 mm  

